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Vaccum Distillation Setup


DESCRIPTION :

The experimental set up consists of a distillation still. The distillation steel is surrounded by another still is constructed of mild steel. The vapour coming from the steel are sucked by means of vaccum pump. only non condensable gases go to the pump while the vapours are condensed by the water called condenser. Water is circulated through the condenser tube . The bottom product from the steel is discharged by means of the bottom drain point while the condensed vapour is discharge by means of the drain.

RANGE OF EXPERIMENTS TO BE CARRIED OUT :

  • To carryout distillation under vaccum.
  • To Verify Rayleigh equation.

EXPERIMENTAL SETUP :

  • Reboiler : Material Stainless Steel
  • Column : Material Stainless Steel
  • Reflux Drum : Material Stainless Steel
  • Condenser : SS , Shell and Tube type Condenser
  • Flow Measurement : 1 No. Pre calibrated Rota meter
  • Packing : Rasching Ring.
  • Heating Mantle : Aluminum body with fiber cloth
  • Digital Temp Indicator : 0 – 400 0 C.
  • Temp Sensor : CR/AL Type
  • Distillate Receiver : Material Stainless Steel
  • Vacuum Pump : Compactable capacity
  • Piping : SS , PVC
  • Setup Mounting : On sturdy MS stand with powder coated

SERVICE REQUIRED :

Water Supply : 2 lpm

Power Supply : 230V, 50Hz, A. C,
Specific Gravity Bottle

CHEMICALS REQUIRED:

Methanol Or Ethanol ,

SPACE REQUIRED :

1.5 m. (L) x 1.0 m(W) X 2.0 m (H)

WEIGHT : @ 65 Kg




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